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Chapter Ⅰ Layered Hydroxide and Oxide Nanocones 1

Layered Cobalt Hydroxide Nanocones：Microwave-Assisted Synthesis,Exfoliation and Structural Modification 3

A General Strategy to Layered Transition-Metal Hydroxide Nanocones：Tuning the Composition for High Electrochemical Performance 17

High-Yield Preparation,Versatile Structural Modification,and Properties of Layered Cobalt Hydroxide Nanocones 34

Layered Zinc Hydroxide Nanocones：Synthesis,Facile Morphological and Structural Modification,and Properties 59

Chapter Ⅱ Inorganic Nanotubes 75

Selective and Controlled Synthesis of Single-Crystalline Yttrium Hydroxide/Oxide Nanosheets and Nanotubes 77

Rational Synthetic Strategy：From ZnO Nanorods to ZnS Nanotubes 96

Selective Synthesis and Magnetic Properties of Uniform CoTe and CoTe2 Nanotubes 110

Shape-Controlled Synthesis and Properties of Manganese Sulfide Microcrystals via a Biomolecule-Assisted Hydrothermal Process 120

Conversion of Metal Oxide Nanosheets into Nanotubes 132

Chapter Ⅲ Cobalt and Nickel Oxide Nanorings 147

Cobalt Hydroxide Nanosheets and Their Thermal Decomposition to Cobalt Oxide Nanorings 149

Rationally Synthetic Strategy：From Nickel Hydroxide Nanosheets to Nickel Oxide Nanorolls 166

Chapter Ⅳ Rare-Earth Oxide and Oxysulfate Hollow Spheres 179

Controllable Fabrication and Optical Properties of Uniform Gadolinium Oxysulfate Hollow Spheres 181

Hollow Spherical Rare-Earth-Doped Yttrium Oxysulfate：A Novel Structure for Upconversion 197

Controlled Fabrication and Optical Properties of Uniform CeO2 Hollow Spheres 213

General Synthetic Strategy for High-Yield and Uniform Rare-Earth Oxysulfates（RE2O2SO4,RE=La,Pr,Nd,Sm,Eu,Gd,Tb,Dy,Y,Ho,and Yb）Hollow Spheres 225

Chapter Ⅴ Transition-Metal Oxide and Chalcogenides Hollow Spheres 241

Controllable Fabrication and Magnetic Properties of Double-Shell Cobalt Oxides Hollow Particles 243

Shape-Controlled Synthesis and Characterization of Cobalt Oxides Hollow Spheres and Octahedra 257

Shape-Controlled Synthesis and Properties of Dandelion-Like Manganese Sulfide Hollow Spheres 274

Nickel Dichalcogenides Hollow Spheres：Controllable Fabrication,Structural Modification and Magnetic Properties 286

Biomolecule-Assisted Hydrothermal Synthesis and Properties of Manganese Sulfide Hollow Microspheres 300

Biomolecule-Assisted Hydrothermal Synthesis and Electrochemical Properties of Copper Sulfide Hollow Spheres 311

Chapter Ⅵ Other Hollow Spheres 323

Hollow Metallic Microspheres：Fabrication and Characterization 325

Selective Synthesis and Properties of Monodisperse Zn Ferrite Hollow Nanospheres and Nanosheets 339

Controllable Fabrication of SiO2/Polypyrrole Core-Shell Particles and Polypyrrole Hollow Spheres 351